{"id":162,"date":"2020-08-25T15:13:27","date_gmt":"2020-08-25T13:13:27","guid":{"rendered":"https:\/\/web.umons.ac.be\/smos\/?p=162"},"modified":"2022-05-23T15:16:36","modified_gmt":"2022-05-23T13:16:36","slug":"new-paper-published-in-polymers-open-access-in-collaboration-with-prof-philippe-zinck-from-the-university-of-lille","status":"publish","type":"post","link":"https:\/\/web.umons.ac.be\/smos\/2020\/08\/25\/new-paper-published-in-polymers-open-access-in-collaboration-with-prof-philippe-zinck-from-the-university-of-lille\/","title":{"rendered":"New paper published in Polymers (open access) in collaboration with Prof Philippe Zinck from the University of Lille."},"content":{"rendered":"
\"New
New paper published in Polymers (open access) in collaboration with Prof Philippe Zinck from the University of Lille.<\/figcaption><\/figure>\n

The paper untitled \u201cEnzymatic Polycondensation of 1,6-Hexanediol and Diethyl Adipate: A Statistical Approach Predicting the Key-Parameters in Solution and in Bulk\u00a0\u00bb Discussed about enzymatic polycondensation of 1,6-hexanediol and diethyl adipate. The influence of various parameters including time, temperature, enzyme loading, and vacuum was assessed in the frame of a two-step polymerization with the help of response surface methodology, a statistical technique that investigates relations between input and output variables. Results in solution (diphenyl ether) and bulk conditions showed that a two-hour reaction time was enough to allow adequate oligomer growth for the first step conducted under atmospheric pressure at 100 \u25e6C. The number-average molecular weight (Mn) achieved varied between 5000 and 12,000 g\u00b7mol\u22121 after a 24 h reaction and up to 18,500 g\u00b7mol\u22121 after 48 h. In this study, mass spectrometry was used in order to characterized the structure of the newly synthetized polymers.<\/p>\n

The full text is available at the following address https:\/\/www.mdpi.com\/2073-4360\/12\/9\/1907<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"

The paper untitled \u201cEnzymatic Polycondensation of 1,6-Hexanediol and Diethyl Adipate: A Statistical Approach Predicting the Key-Parameters in Solution and in Bulk\u00a0\u00bb Discussed about enzymatic polycondensation of 1,6-hexanediol and diethyl adipate.<\/p>\n","protected":false},"author":157,"featured_media":163,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[47],"tags":[],"class_list":["post-162","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-recherche"],"yoast_head":"\nNew paper published in Polymers (open access) in collaboration with Prof Philippe Zinck from the University of Lille. - Service \/ FS - Synth\u00e8se et Spectrom\u00e9trie de Masse Organiques<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/web.umons.ac.be\/smos\/2020\/08\/25\/new-paper-published-in-polymers-open-access-in-collaboration-with-prof-philippe-zinck-from-the-university-of-lille\/\" \/>\n<meta property=\"og:locale\" content=\"fr_FR\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"New paper published in Polymers (open access) in collaboration with Prof Philippe Zinck from the University of Lille. - 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